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Organic Laboratory Techniques by Ralph J. Fessenden, Jess Feist, Joan S. Fessenden and Patty Feist (2000, Trade Paperback)
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About this product
Product Identifiers
PublisherBrooks/Cole
ISBN-100534379818
ISBN-139780534379810
eBay Product ID (ePID)1734540
Product Key Features
Number of Pages256 Pages
Publication NameOrganic Laboratory Techniques
LanguageEnglish
Publication Year2000
SubjectGeneral, Chemistry / Organic
FeaturesRevised
TypeTextbook
AuthorRalph J. Fessenden, Jess Feist, Joan S. Fessenden, Patty Feist
Subject AreaScience, Education
FormatTrade Paperback
Dimensions
Item Height0.5 in
Item Weight14.4 Oz
Item Length9.3 in
Item Width7.4 in
Additional Product Features
Edition Number3
Intended AudienceCollege Audience
LCCN00-033718
ReviewsINTRODUCTION TO THE ORGANIC LABORATORYSafety in the Laboratory / The Laboratory Notebook / Laboratory Equipment1. CRYSTALLIZATIONSolvents for Crystallization / Steps in Crystallization / Supplemental Procedures2. MELTING POINTSCharacteristics of Melting Points / Melting-Point Apparatus / Steps in Determining a Melting Point / Supplemental Procedures3. EXTRACTIONImmiscible Liquids / Distribution Coefficients / Extraction Solvents / Chemically Active Extraction / Steps in Extractions / Additional Techniques Used in Extractions / Other Extraction Techniques4. DRYING ORGANIC SOLUTIONSExtraction with Aqueous Sodium Chloride / Solid Inorganic Drying Agents / Procedure for Using Solid Inorganic Drying Agents / Azeotropic Drying5. SIMPLE DISTILLATIONCharacteristics of Distillation / Steps in a Simple Distillation / Microscale and Semi-Microscale Distillation6. FRACTIONAL DISTILLATIONEfficiency of the Fractionation Column / Steps in Fractional Distillation / Microscale Fractional Distillation7. VACUUM DISTILLATIONBoiling Point and Pressure / Apparatus for Simple Vacuum Distillation / Steps in Vacuum Distillation8. STEAM DISTILLATIONCharacteristics of Steam Distillation / Calculation of the Amount of Water Needed in a Steam Distillation / Apparatus for Steam Distillation9. SUBLIMATIONAtmospheric Sublimation / Vacuum Sublimation10. REFRACTIVE INDEXCorrecting for Temperature Differences / Steps in Using a Refractometer11. COLUMN CHROMATOGRAPHYGravity Column Chromatography. Flash Chromatography (Macroscale) / Flash Chromatography (Microscale) / High-Performance Liquid Chromatography (HPLC)12. THIN LAYER CHROMATOGRAPHYThe RF Value / Equipment for TLC / Steps in a TLC Analysis / A Related Technique: Paper Chromatography13. GAS CHROMATOGRAPHYGas Chromatography / The Gas Chromatograph / Steps in a GC Analysis / Problems Encountered in GC / Uses of Gas Chromatograms14. CARRYING OUT TYPICAL REACTIONSStirring / Heating Reaction Mixtures / Controlling Exothermic Reactions / Adding Reagents to a Reaction Mixture. Excluding Moisture from a Reaction Mixture / Setting Up a Three-Neck Reaction Flask / Hydrogen Halide Gas Traps15. INFRARED SPECTROSCOPYThe Infrared Spectrum / Absorption of Infrared Radiation / Interpreting Infrared Spectra / Identifying Types of Compounds / Preparing a Sample for an Infrared Spectrum / Instrumentation16. PROTON NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYThe NMR Spectrum / Interpreting NMR Spectra / Use of Deuterium in Proton NMR Spectroscopy / NMR Spectra of Unknowns / The NMR Spectrometer / Preparing Samples for NMR Spectra17. THE CHEMICAL LITERATUREIntroduction to the Chemical Literature / Secondary Literature / Primary Literature / APPENDIX I. COMMONLY USED CALCULATIONS / Molarity / Normality / Dilutions / Percent Concentrations / Percent Yields and Theoretical Yields / APPENDIX II / ELEMENTAL ANALYSES / Determining the Empirical Formula / Determining the Molecular Formula / Interpreting the Results of Elemental Analysis / Degree of Unsaturation / APPENDIX III. HEALTH HAZARDS OF COMPOUNDS USED IN ORGANIC CHEMISTRY / Where to Find Chemical Hazard Information / Understanding Health Hazard Warnings
Dewey Edition21
IllustratedYes
Dewey Decimal547/.0078
Edition DescriptionRevised edition
Table Of ContentINTRODUCTION TO THE ORGANIC LABORATORYSafety in the Laboratory / The Laboratory Notebook / Laboratory Equipment1. CRYSTALLIZATIONSolvents for Crystallization / Steps in Crystallization / Supplemental Procedures2. MELTING POINTSCharacteristics of Melting Points / Melting-Point Apparatus / Steps in Determining a Melting Point / Supplemental Procedures3. EXTRACTIONImmiscible Liquids / Distribution Coefficients / Extraction Solvents / Chemically Active Extraction / Steps in Extractions / Additional Techniques Used in Extractions / Other Extraction Techniques4. DRYING ORGANIC SOLUTIONSExtraction with Aqueous Sodium Chloride / Solid Inorganic Drying Agents / Procedure for Using Solid Inorganic Drying Agents / Azeotropic Drying5. SIMPLE DISTILLATIONCharacteristics of Distillation / Steps in a Simple Distillation / Microscale and Semi-Microscale Distillation6. FRACTIONAL DISTILLATIONEfficiency of the Fractionation Column / Steps in Fractional Distillation / Microscale Fractional Distillation7. VACUUM DISTILLATIONBoiling Point and Pressure / Apparatus for Simple Vacuum Distillation / Steps in Vacuum Distillation8. STEAM DISTILLATIONCharacteristics of Steam Distillation / Calculation of the Amount of Water Needed in a Steam Distillation / Apparatus for Steam Distillation9. SUBLIMATIONAtmospheric Sublimation / Vacuum Sublimation10. REFRACTIVE INDEXCorrecting for Temperature Differences / Steps in Using a Refractometer11. COLUMN CHROMATOGRAPHYGravity Column Chromatography. Flash Chromatography (Macroscale) / Flash Chromatography (Microscale) / High-Performance Liquid Chromatography (HPLC)12. THIN LAYER CHROMATOGRAPHYThe RF Value / Equipment for TLC / Steps in a TLC Analysis / A Related Technique: Paper Chromatography13. GAS CHROMATOGRAPHYGas Chromatography / The Gas Chromatograph / Steps in a GC Analysis / Problems Encountered in GC / Uses of Gas Chromatograms14. CARRYING OUT TYPICAL REACTIONSStirring / Heating Reaction Mixtures / Controlling Exothermic Reactions / Adding Reagents to a Reaction Mixture. Excluding Moisture from a Reaction Mixture / Setting Up a Three-Neck Reaction Flask / Hydrogen Halide Gas Traps15. INFRARED SPECTROSCOPYThe Infrared Spectrum / Absorption of Infrared Radiation / Interpreting Infrared Spectra / Identifying Types of Compounds / Preparing a Sample for an Infrared Spectrum / Instrumentation16. PROTON NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYThe NMR Spectrum / Interpreting NMR Spectra / Use of Deuterium in Proton NMR Spectroscopy / NMR Spectra of Unknowns / The NMR Spectrometer / Preparing Samples for NMR Spectra17. THE CHEMICAL LITERATUREIntroduction to the Chemical Literature / Secondary Literature / Primary Literature / APPENDIX I. COMMONLY USED CALCULATIONS / Molarity / Normality / Dilutions / Percent Concentrations / Percent Yields and Theoretical Yields / APPENDIX II / ELEMENTAL ANALYSES / Determining the Empirical Formula / Determining the Molecular Formula / Interpreting the Results of Elemental Analysis / Degree of Unsaturation / APPENDIX III. HEALTH HAZARDS OF COMPOUNDS USED IN ORGANIC CHEMISTRY / Where to Find Chemical Hazard Information / Understanding Health Hazard Warnings
SynopsisThis highly effective and practical manual is designed to be used as a supplementary text for the organic chemistry laboratory course - and with virtually any main text - in which experiments are supplied by the instructor or in which the students work independently. Each technique contains a brief theoretical discussion. Steps used in each technique, along with common problems that might arise. These respected and renowned authors include supplemental or related procedures, suggested experiments, and suggested readings for many of the techniques. Additionally, each chapter ends with a set of study problems that primarily stress the practical aspects of each technique, and microscale techniques are included throughout the text, as appropriate. Additional exercises, reference material, and quizzes are available online.
LC Classification NumberQD261.F466 2000
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