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Organic Laboratory Techniques by Joan S. Fessenden, Ralph J. Fessenden, Patty Feist and Jess Feist (2000, Trade Paperback, Revised edition)

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This textbook titled "Organic Laboratory Techniques" is an excellent resource for those involved in organic chemistry. The book is authored by Ralph J. Fessenden, Jess Feist, Joan S. Fessenden, and Patty Feist and was published in 2000 by Brooks/Cole.

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Product Information

This highly effective and practical manual is designed to be used as a supplementary text for the organic chemistry laboratory course - and with virtually any main text - in which experiments are supplied by the instructor or in which the students work independently. Each technique contains a brief theoretical discussion. Steps used in each technique, along with common problems that might arise. These respected and renowned authors include supplemental or related procedures, suggested experiments, and suggested readings for many of the techniques. Additionally, each chapter ends with a set of study problems that primarily stress the practical aspects of each technique, and microscale techniques are included throughout the text, as appropriate. Additional exercises, reference material, and quizzes are available online.

Product Identifiers

Publisher
Brooks/Cole
ISBN-10
0534379818
ISBN-13
9780534379810
eBay Product ID (ePID)
1734540

Product Key Features

Author
Ralph J. Fessenden, Jess Feist, Joan S. Fessenden, Patty Feist
Publication Name
Organic Laboratory Techniques
Format
Trade Paperback
Language
English
Features
Revised
Publication Year
2000
Type
Textbook
Number of Pages
256 Pages

Dimensions

Item Length
9.3in
Item Height
0.5in
Item Width
7.4in
Item Weight
14.4 Oz

Additional Product Features

Lc Classification Number
Qd261.F466 2000
Edition Description
Revised Edition
Edition Number
3
Reviews
INTRODUCTION TO THE ORGANIC LABORATORYSafety in the Laboratory / The Laboratory Notebook / Laboratory Equipment1. CRYSTALLIZATIONSolvents for Crystallization / Steps in Crystallization / Supplemental Procedures2. MELTING POINTSCharacteristics of Melting Points / Melting-Point Apparatus / Steps in Determining a Melting Point / Supplemental Procedures3. EXTRACTIONImmiscible Liquids / Distribution Coefficients / Extraction Solvents / Chemically Active Extraction / Steps in Extractions / Additional Techniques Used in Extractions / Other Extraction Techniques4. DRYING ORGANIC SOLUTIONSExtraction with Aqueous Sodium Chloride / Solid Inorganic Drying Agents / Procedure for Using Solid Inorganic Drying Agents / Azeotropic Drying5. SIMPLE DISTILLATIONCharacteristics of Distillation / Steps in a Simple Distillation / Microscale and Semi-Microscale Distillation6. FRACTIONAL DISTILLATIONEfficiency of the Fractionation Column / Steps in Fractional Distillation / Microscale Fractional Distillation7. VACUUM DISTILLATIONBoiling Point and Pressure / Apparatus for Simple Vacuum Distillation / Steps in Vacuum Distillation8. STEAM DISTILLATIONCharacteristics of Steam Distillation / Calculation of the Amount of Water Needed in a Steam Distillation / Apparatus for Steam Distillation9. SUBLIMATIONAtmospheric Sublimation / Vacuum Sublimation10. REFRACTIVE INDEXCorrecting for Temperature Differences / Steps in Using a Refractometer11. COLUMN CHROMATOGRAPHYGravity Column Chromatography. Flash Chromatography (Macroscale) / Flash Chromatography (Microscale) / High-Performance Liquid Chromatography (HPLC)12. THIN LAYER CHROMATOGRAPHYThe RF Value / Equipment for TLC / Steps in a TLC Analysis / A Related Technique: Paper Chromatography13. GAS CHROMATOGRAPHYGas Chromatography / The Gas Chromatograph / Steps in a GC Analysis / Problems Encountered in GC / Uses of Gas Chromatograms14. CARRYING OUT TYPICAL REACTIONSStirring / Heating Reaction Mixtures / Controlling Exothermic Reactions / Adding Reagents to a Reaction Mixture. Excluding Moisture from a Reaction Mixture / Setting Up a Three-Neck Reaction Flask / Hydrogen Halide Gas Traps15. INFRARED SPECTROSCOPYThe Infrared Spectrum / Absorption of Infrared Radiation / Interpreting Infrared Spectra / Identifying Types of Compounds / Preparing a Sample for an Infrared Spectrum / Instrumentation16. PROTON NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYThe NMR Spectrum / Interpreting NMR Spectra / Use of Deuterium in Proton NMR Spectroscopy / NMR Spectra of Unknowns / The NMR Spectrometer / Preparing Samples for NMR Spectra17. THE CHEMICAL LITERATUREIntroduction to the Chemical Literature / Secondary Literature / Primary Literature / APPENDIX I. COMMONLY USED CALCULATIONS / Molarity / Normality / Dilutions / Percent Concentrations / Percent Yields and Theoretical Yields / APPENDIX II / ELEMENTAL ANALYSES / Determining the Empirical Formula / Determining the Molecular Formula / Interpreting the Results of Elemental Analysis / Degree of Unsaturation / APPENDIX III. HEALTH HAZARDS OF COMPOUNDS USED IN ORGANIC CHEMISTRY / Where to Find Chemical Hazard Information / Understanding Health Hazard Warnings
Table of Content
INTRODUCTION TO THE ORGANIC LABORATORYSafety in the Laboratory / The Laboratory Notebook / Laboratory Equipment1. CRYSTALLIZATIONSolvents for Crystallization / Steps in Crystallization / Supplemental Procedures2. MELTING POINTSCharacteristics of Melting Points / Melting-Point Apparatus / Steps in Determining a Melting Point / Supplemental Procedures3. EXTRACTIONImmiscible Liquids / Distribution Coefficients / Extraction Solvents / Chemically Active Extraction / Steps in Extractions / Additional Techniques Used in Extractions / Other Extraction Techniques4. DRYING ORGANIC SOLUTIONSExtraction with Aqueous Sodium Chloride / Solid Inorganic Drying Agents / Procedure for Using Solid Inorganic Drying Agents / Azeotropic Drying5. SIMPLE DISTILLATIONCharacteristics of Distillation / Steps in a Simple Distillation / Microscale and Semi-Microscale Distillation6. FRACTIONAL DISTILLATIONEfficiency of the Fractionation Column / Steps in Fractional Distillation / Microscale Fractional Distillation7. VACUUM DISTILLATIONBoiling Point and Pressure / Apparatus for Simple Vacuum Distillation / Steps in Vacuum Distillation8. STEAM DISTILLATIONCharacteristics of Steam Distillation / Calculation of the Amount of Water Needed in a Steam Distillation / Apparatus for Steam Distillation9. SUBLIMATIONAtmospheric Sublimation / Vacuum Sublimation10. REFRACTIVE INDEXCorrecting for Temperature Differences / Steps in Using a Refractometer11. COLUMN CHROMATOGRAPHYGravity Column Chromatography. Flash Chromatography (Macroscale) / Flash Chromatography (Microscale) / High-Performance Liquid Chromatography (HPLC)12. THIN LAYER CHROMATOGRAPHYThe RF Value / Equipment for TLC / Steps in a TLC Analysis / A Related Technique: Paper Chromatography13. GAS CHROMATOGRAPHYGas Chromatography / The Gas Chromatograph / Steps in a GC Analysis / Problems Encountered in GC / Uses of Gas Chromatograms14. CARRYING OUT TYPICAL REACTIONSStirring / Heating Reaction Mixtures / Controlling Exothermic Reactions / Adding Reagents to a Reaction Mixture. Excluding Moisture from a Reaction Mixture / Setting Up a Three-Neck Reaction Flask / Hydrogen Halide Gas Traps15. INFRARED SPECTROSCOPYThe Infrared Spectrum / Absorption of Infrared Radiation / Interpreting Infrared Spectra / Identifying Types of Compounds / Preparing a Sample for an Infrared Spectrum / Instrumentation16. PROTON NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYThe NMR Spectrum / Interpreting NMR Spectra / Use of Deuterium in Proton NMR Spectroscopy / NMR Spectra of Unknowns / The NMR Spectrometer / Preparing Samples for NMR Spectra17. THE CHEMICAL LITERATUREIntroduction to the Chemical Literature / Secondary Literature / Primary Literature / APPENDIX I. COMMONLY USED CALCULATIONS / Molarity / Normality / Dilutions / Percent Concentrations / Percent Yields and Theoretical Yields / APPENDIX II / ELEMENTAL ANALYSES / Determining the Empirical Formula / Determining the Molecular Formula / Interpreting the Results of Elemental Analysis / Degree of Unsaturation / APPENDIX III. HEALTH HAZARDS OF COMPOUNDS USED IN ORGANIC CHEMISTRY / Where to Find Chemical Hazard Information / Understanding Health Hazard Warnings
Copyright Date
2001
Target Audience
College Audience
Topic
General, Chemistry / Organic
Lccn
00-033718
Dewey Decimal
547/.0078
Dewey Edition
21
Illustrated
Yes
Genre
Education, Science

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4.3

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Most relevant reviews

4 out of 5 stars
by dervjm6Mar 07, 2010
Awexome
I really like it. It is very descriptive with all the different techniques that are discussed. I read it every week before my lab and It helps me on my lab quizzes.
4 out of 5 stars
by aceHIO1cQmu@Del...Jan 29, 2009
Organic Laboratory Techniques review
The book basically covers most of organic laboratory techniques. Diagrams help and the book is pretty good overall.

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