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Synthesis of Branched Alpha- and Beta-Amino Acids. Using C-Nucleophile Additions
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Item specifics
- Condition
- ISBN-13
- 9783832523268
- Book Title
- Synthesis of Branched Alpha- and Beta-Amino Acids. Using C-Nucl
- ISBN
- 9783832523268
- Subject Area
- Science
- Publication Name
- Synthesis of Branched Alpha- And Beta-Amino Acids : Using C-Nucleophile Additions to Imines and Nitrones
- Publisher
- Logos Verlag Berlin
- Item Length
- 8.3 in
- Subject
- Chemistry / General
- Publication Year
- 2009
- Type
- Textbook
- Format
- Trade Paperback
- Language
- English
- Item Weight
- 19.7 Oz
- Item Width
- 5.7 in
- Number of Pages
- 230 Pages
About this product
Product Identifiers
Publisher
Logos Verlag Berlin
ISBN-10
383252326X
ISBN-13
9783832523268
eBay Product ID (ePID)
17038404159
Product Key Features
Number of Pages
230 Pages
Publication Name
Synthesis of Branched Alpha- And Beta-Amino Acids : Using C-Nucleophile Additions to Imines and Nitrones
Language
English
Publication Year
2009
Subject
Chemistry / General
Type
Textbook
Subject Area
Science
Format
Trade Paperback
Dimensions
Item Weight
19.7 Oz
Item Length
8.3 in
Item Width
5.7 in
Additional Product Features
Intended Audience
College Audience
Synopsis
Artificial peptides, containing alpha- and/or beta-amino acids with bulky substituents, can potentially possess some unusual properties, for example, decreased conformational ability or formation of stable secondary structures. Therefore, the preparation of such unnatural amino acids is of high interest. In this thesis, a route to enantiomerically pure 1-adamantylglycine was developed. The crucial step was the highly stereoselective addition of adamantylmagnesium bromide to the C=N bond of 2,3-O-cyclohexylidene-D-glyceraldehyde N-benzylnitrone effected in the presence of Lewis acid. Finally, 1-adamantylglycine was synthesized in 28 % yield over 6 steps. The routes to 9-aminofluorenylacetic and beta-aminobeta, beta-diphenylpropionic acids were proposed and they consist in the addition of allyl Grignard reagents to imines with various protecting groups, followed by oxidative transformation of the allyl group. Also some procedures for the preparation of 3,3-disubstituted 4-azetidinones, direct precursors of the corresponding beta-branched beta-amino acids, have been investigated.
Item description from the seller
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- t***u (123)- Feedback left by buyer.Past monthVerified purchaseThe book was in excellent condition, quality and appearance excellent as described, and packaged safely in a box very well. Seller shipped immediately and communication and payment transfer was excellent. Great eBayer!!! Price of book was very competitive. A+++++
- w***8 (7)- Feedback left by buyer.Past 6 monthsVerified purchaseThe book came exactly as described and packaged well. The shipping time was long but not unfair. I had some issues tracking but contacted the seller and they were responsive and accommodating. Great price and quality and I will be purchasing again if possible! Cheers!The Outcast Dead by Graham McNeill (English) Paperback Book (#395751902743)
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